Ishdan maqsad 3-amino-5-merkapto-1,2,4-triazoldan yangi organik modda 3,3'-disulfanidilbis(1H-1,2,4-triazol-5-amin)ni sintez qilishdir. Maqolada 3-amino-5-merkapto-1,2,4-triazolning ahamiyati va undan 3,3'-disulfanidilbis(1H-1,2,4-triazol-5-amin)ning eng maqbul sintez usuli keltirilgan. 3-amino-5-merkapto-1,2,4-triazol va 3,3'-disulfanidilbis(1H-1,2,4-triazol-5-amin)ning infraqizil va Raman spektroskopik tahlillari keltirilgan.
Ishdan maqsad 3-amino-5-merkapto-1,2,4-triazoldan yangi organik modda 3,3'-disulfanidilbis(1H-1,2,4-triazol-5-amin)ni sintez qilishdir. Maqolada 3-amino-5-merkapto-1,2,4-triazolning ahamiyati va undan 3,3'-disulfanidilbis(1H-1,2,4-triazol-5-amin)ning eng maqbul sintez usuli keltirilgan. 3-amino-5-merkapto-1,2,4-triazol va 3,3'-disulfanidilbis(1H-1,2,4-triazol-5-amin)ning infraqizil va Raman spektroskopik tahlillari keltirilgan.
Цель работы – синтез нового органического вещества 3,3'-дисульфанидилбис(1Н-1,2,4-триазол-5-амина) из 3-амино-5-меркапто-1,2,4-триазола. В статье представлены оптимальный метод синтеза 3,3'-дисульфанидилбис(1Н-1,2,4-триазол-5-амина) из 3-амино-5-меркапто-1,2,4-триазола и его значение. Представлены результаты инфракрасного и рамановского спектроскопического анализа 3-амино-5-меркапто-1,2,4-триазола и 3,3'-дисульфанидилбис(1Н-1,2,4-триазол-5-амина).
The aim of this work is the synthesis of a new organic compound 3,3'-disulfanidylbis(1Н-1,2,4-triazole-5-amine) from 3-amino-5-mercapto-1,2,4-triazole. The article presents the optimal method for the synthesis of 3,3'-disulfanidylbis(1Н-1,2,4-triazole-5-amine) from 3-amino-5-mercapto-1,2,4-triazole and its significance. The results of infrared and Raman spectroscopic analysis of 3-amino-5-mercapto-1,2,4-triazole and 3,3'-disulfanidylbis(1H-1,2,4-triazole-5-amine) are presented.
№ | Muallifning F.I.Sh. | Lavozimi | Tashkilot nomi |
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1 | Xayrullayev G.U. | 1 | National University of Uzbekistan |
2 | Kadirova S.A. | 2 | National University of Uzbekistan |
3 | Torambetov B.S. | 3 | National University of Uzbekistan |
4 | Botirova S.A. | 4 | National University of Uzbekistan |
5 | Mavlonova S.R. | 5 | National University of Uzbekistan |
№ | Havola nomi |
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1 | 1. A. Kamal, MA. Syed, & SM. Mohammed. “Theraputic Potential of Benzothaizole” A Patent Review (2010- 2104). Informa healthcare, 25 (3), 2015. |
2 | 2. AK. Singh, & KR. Kandel, “Synthesis of Triazole Derivative: [4-(Benzylideneamino)-5-phenyl-4H-1,2,4- triazole-3-thiol],” J. Nepal Chem. Soc., 30, 2012. |
3 | 3. Артемьев Г.А., Уломский Е.Н., Русинов В.Л. “Оптимизация промышленных методов получения 5-амино-3-меркапто-1,2,4-триазола и 5-амино-3-метилтио-1,2,4-триазола” |
4 | 4. Frank Hipler, Manuela Winter, Roland A. Fischer N–S–H hydrogen bonding in 2-mercapto-5-methyl-1,3,4-thiadiazole. Synthesis and crystal structures of mercapto functionalised 1,3,4-thiadiazoles. |
5 | 5. Potts K.T. The chemistry of 1,2,4-triazoles. |
6 | 6. Yanli Gai, Xitong Chen, Huajun Yang, Yanxiang Wang, Xianhui Bu A new strategy for constructing a disulfidefunctionalized ZIF-8 analogue using structuredirecting ligand–ligand covalent interaction. |
7 | 7. K. Bahgat, & S. Fraihat, “Normal Coordinate Analysis, Molecular Structure, Vibrational, Electronic Spectra and NMR Investigation of 4-Amino-3-phenyl-1H-1,2,4- triazole-5(4H)-thione by Ab initio HF and DFT Method,” Spectrochimica Acta Part A: Mol. Biomol. Spectro., 135, 2015. |
8 | 8. А. В. Васильев, Е. В. Гриненко, А. О. Щукин, Т. Г. Федулина Инфракрасная спектроскопия органических и природных соединений. САНКТ-ПЕТЕРБУРГ СПбГЛТА 2007. Ст-16. |